Chemical Processing - September 2007 - (Page 61) >> PROCESS PUZZLER PROCESS PUZZLER < > THIS MONTH’S PUZZLER Our clean-in-place (CIP) system now involves a hot water rinse, followed by a caustic rinse, followed by a biocide in a phosphoric acid solution. The new owners of the plant want to make a change. They propose switching the acid rinse to a steam sterilization step at about 230°F. We are worried about the mechanical seals in process pumps. The pump vendor doesn’t recommend the seals above 225°F and also is concerned about the effect on bearings and pump performance. Do you think agitator seals also will be affected? What improvements do you think are needed to comply with our new owners’ wishes without extensive changes throughout the plant? Keep an acid rinse I would recommend keeping an acid rinse followed by steam sanitization at 220°F. The acid rinse would not only kill organisms but neutralize the residual caustic and dissolve its salt deposits. I wouldn’t recommend keeping the phosphoric acid but rather use of a different acid with biocide. Phosphorous is a key building block in phospholipids formation in the cell membranes/walls of microorganisms. It actually aids in making acid-adapted microorganisms more viable, which could lead to undesirable proliferation. Also, I would be wary of phosphorous polymerizing in the presence of salt deposits in the heat exchanger, leaving behind a pseudo-biofilm on internal surfaces. Biofilms can thermally insulate microorganisms. Be wary of the term sterilization versus sanitization. Sterilization occurs above 250°F as a function of time and heat penetration, at which you’ll be in the killing zone for critical pathogens (e.g., c.botulinum, e. coli). Other thermophilic organisms may survive but are typically non-pathogenic. Of course, since you’re fermenting, microorganism proliferation should be minimal due to competing factors of the organism you’re trying to grow. Ron Johnson, principal engineer PepsiCo, Valhalla, N.Y. Answer other questions first The Puzzler seems to raise more questions that need to be answered before a definitive answer to the question can be given. The first question is why sterilize at 230°F (110°C)? Presumably the new owners wish to eliminate the possibilwww.chemicalprocessing.com http://www.chemicalprocessing.com
Table of Contents Feed for the Digital Edition of Chemical Processing - September 2007 Contents From the Editor Field Notes In Process Energy Saver Compliance Advisor Succeed at Simulation Rethink Your Approach to Process Safety Avoid Blending Blunders Get the Right Cartridge or Bag Filter Wireless Proponents Take HART Membrane Boasts Material Benefits Process Puzzler Plant InSites Chem Show Product Preview ISA Product Preview Equipment & Services Product Spotlight/Classifieds Ad Index End Point Chemical Processing - September 2007 Chemical Processing - September 2007 - (Page Cover1) Chemical Processing - September 2007 - (Page Cover2) Chemical Processing - September 2007 - (Page 3) Chemical Processing - September 2007 - (Page 4) Chemical Processing - September 2007 - Contents (Page 5) Chemical Processing - September 2007 - Contents (Page 6) Chemical Processing - September 2007 - From the Editor (Page 7) Chemical Processing - September 2007 - From the Editor (Page 8) Chemical Processing - September 2007 - From the Editor (Page 9) Chemical Processing - September 2007 - From the Editor (Page 10) Chemical Processing - September 2007 - Field Notes (Page 11) Chemical Processing - September 2007 - Field Notes (Page 12) Chemical Processing - September 2007 - Field Notes (Page 13) Chemical Processing - September 2007 - Field Notes (Page 14) Chemical Processing - September 2007 - In Process (Page 15) Chemical Processing - September 2007 - In Process (Page 16) Chemical Processing - September 2007 - In Process (Page 17) Chemical Processing - September 2007 - In Process (Page 18) Chemical Processing - September 2007 - Energy Saver (Page 19) Chemical Processing - September 2007 - Energy Saver (Page 20) Chemical Processing - September 2007 - Compliance Advisor (Page 21) Chemical Processing - September 2007 - Compliance Advisor (Page 22) Chemical Processing - September 2007 - Compliance Advisor (Page 23) Chemical Processing - September 2007 - Compliance Advisor (Page 24) Chemical Processing - September 2007 - Compliance Advisor (Page 25) Chemical Processing - September 2007 - Compliance Advisor (Page 26) Chemical Processing - September 2007 - Compliance Advisor (Page 27) Chemical Processing - September 2007 - Compliance Advisor (Page 28) Chemical Processing - September 2007 - Compliance Advisor (Page 29) Chemical Processing - September 2007 - Compliance Advisor (Page 30) Chemical Processing - September 2007 - Succeed at Simulation (Page 31) Chemical Processing - September 2007 - Succeed at Simulation (Page 32) Chemical Processing - September 2007 - Succeed at Simulation (Page 33) Chemical Processing - September 2007 - Succeed at Simulation (Page 34) Chemical Processing - September 2007 - Succeed at Simulation (Page 35) Chemical Processing - September 2007 - Rethink Your Approach to Process Safety (Page 36) Chemical Processing - September 2007 - Rethink Your Approach to Process Safety (Page 37) Chemical Processing - September 2007 - Rethink Your Approach to Process Safety (Page 38) Chemical Processing - September 2007 - Rethink Your Approach to Process Safety (Page 39) Chemical Processing - September 2007 - Rethink Your Approach to Process Safety (Page 40) Chemical Processing - September 2007 - Rethink Your Approach to Process Safety (Page 41) Chemical Processing - September 2007 - Avoid Blending Blunders (Page 42) Chemical Processing - September 2007 - Avoid Blending Blunders (Page 43) Chemical Processing - September 2007 - Avoid Blending Blunders (Page 44) Chemical Processing - September 2007 - Avoid Blending Blunders (Page 45) Chemical Processing - September 2007 - Avoid Blending Blunders (Page 46) Chemical Processing - September 2007 - Avoid Blending Blunders (Page 47) Chemical Processing - September 2007 - Avoid Blending Blunders (Page 48) Chemical Processing - September 2007 - Avoid Blending Blunders (Page 49) Chemical Processing - September 2007 - Get the Right Cartridge or Bag Filter (Page 50) Chemical Processing - September 2007 - Get the Right Cartridge or Bag Filter (Page 51) Chemical Processing - September 2007 - Get the Right Cartridge or Bag Filter (Page 52) Chemical Processing - September 2007 - Get the Right Cartridge or Bag Filter (Page 53) Chemical Processing - September 2007 - Wireless Proponents Take HART (Page 54) Chemical Processing - September 2007 - Wireless Proponents Take HART (Page 55) Chemical Processing - September 2007 - Wireless Proponents Take HART (Page 56) Chemical Processing - September 2007 - Wireless Proponents Take HART (Page 57) Chemical Processing - September 2007 - Membrane Boasts Material Benefits (Page 58) Chemical Processing - September 2007 - Membrane Boasts Material Benefits (Page 59) Chemical Processing - September 2007 - Membrane Boasts Material Benefits (Page 60) Chemical Processing - September 2007 - Process Puzzler (Page 61) Chemical Processing - September 2007 - Process Puzzler (Page 62) Chemical Processing - September 2007 - Plant InSites (Page 63) Chemical Processing - September 2007 - Chem Show Product Preview (Page 64) Chemical Processing - September 2007 - Chem Show Product Preview (Page 65) Chemical Processing - September 2007 - Chem Show Product Preview (Page 66) Chemical Processing - September 2007 - ISA Product Preview (Page 67) Chemical Processing - September 2007 - Equipment & Services (Page 68) Chemical Processing - September 2007 - Product Spotlight/Classifieds (Page 69) Chemical Processing - September 2007 - Product Spotlight/Classifieds (Page 70) Chemical Processing - September 2007 - Product Spotlight/Classifieds (Page 71) Chemical Processing - September 2007 - Product Spotlight/Classifieds (Page 72) Chemical Processing - September 2007 - Ad Index (Page 73) Chemical Processing - September 2007 - End Point (Page 74) Chemical Processing - September 2007 - End Point (Page Cover3) Chemical Processing - September 2007 - End Point (Page Cover4)
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